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Nov 09, 2021 · The HS-SDME extraction procedure is shown in Fig. 1D. Firstly, 30 mg of the matrix modifier (Na 2 CO 3: Na 2 SO 4 = 3:2, m/m) was placed evenly over the bottom of an 18 mL threaded headspace vial (bottom diameter: 2 cm), which covered ¼ space of the bottom. Then, 10 µL of the test sample or test standard was added to the

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