28/10/1988 · Gas chromatography of fluoroalkyLs'ilane derivatives A 500-/11 side-hole gas-tight syringe (Hamilton, Reno, NV, U.S.A.) was used to sample the headspace of the sample vial. A 12 m x 250 #m I.D. SE-30 capillary column (Scientific Glass Engineering, Austin, TX, U.S.A.) was used in a HP A gas chromatograph, equipped with a FID detector (Hewlett-Packard, Avondale, PA, U.S.A.).