网页Embodiment 1: In the 1 liter of reaction flask that has stirrer, thermometer, airway, add entry 360ml, five water Sulfothiorine 100g, to molten entirely,, dropwise in 20~25 ℃ of dropping methyl-sulfate 50.4g, be cooled to 10 ℃, add ether 100ml, import chlorine 100g, reaction finishes, tell organic layer, the Calcium Chloride Powder