5.3 Automatic headspace sampler. headspace bottle (22 ml), gasket (polytetrafluoroethylene/silicone material), cap (screw cap or Once used glands). 5.4 reciprocating oscillator. oscillation frequency 150 times/min, can be fixed head empty bottle. 5.5 Balance. Accuracy 0.01 g. 5.6 Microinjector. 5 μl, 10 μl, 25 μl, 100 μl, 500 μl.