Nov 25, 2002 · Gas chromatography conditionsThe column was a DB 1701, 30 m×0.25 mm×0.25 μm film thickness (J&W Scientific, Folsom, CA, USA). Helium with a flow-rate of 0.72 ml/min was used as the carrier gas. Nitrogen was the make-up gas for the ECD and had a flow-rate of 60 ml/min. Injection port and detector temperatures were 220 and 250 °C