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Determination of Ethyl Carbamate in Alcoholic Beverages and
Determination of Ethyl Carbamate in Alcoholic Beverages and

Mar 21, 2022 · After 4 min of equilibration, EC was eluted with 160 mL of methylene chloride at a rate of 1 drop per second. The eluent was concentrated to about 2~3 mL using a rotary evaporator, transferred into v-vial, and further concentrated to 1 mL under a gentle stream of nitrogen. Each sample was extracted and analyzed by GC-MS in triplicate.

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Plants | Free Full-Text | Impact of Rootstock and Season on
Plants | Free Full-Text | Impact of Rootstock and Season on

Jul 31, 2021 · The samples were then centrifuged at 3220× g at 4 °C for 15 min. Samples were analyzed in duplicate by transferring two-8 mL portions of supernatant to 20 mL amber headspace vials (Aijiren Technologies, Santa Clara, CA, USA) containing 3 g of NaCl. Each vial was spiked with 50 µL of a 10 mg/L 2-undecanone internal standard solution.

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In-situ derivatization and headspace solid-phase
In-situ derivatization and headspace solid-phase

Apr 08, 2019 · Various parameters like fiber type, headspace time, temperature, and amount of BSTFA were optimized. Under the optimized conditions, the relative standard deviations (RSDs) were in the range 7.0-13.1% and the limits of detection (LODs) were measured to be between 10 and 20 pg mL-1. The application of the developed method was tested using the

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(PDF) Headspace gas chromatography-mass spectrometry method
(PDF) Headspace gas chromatography-mass spectrometry method

mL of the sample solution into 22 mL headspace vial, which was in a tube holder placed on an icebox with an appropriate size. Then, 1 mL of 1 M H 2 SO 4 was added above the cold sample.

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Evaluation of a GC–MS method for benzyl chloride content in
Evaluation of a GC–MS method for benzyl chloride content in

Feb 08, 2022 · For the static headspace (SHS) analysis, 20-mL headspace vials (23 × 75 mm for CTC PAL) and 20-mm crimp caps (w/3-mm thick PTFE/silicone septa, ultralow bleed, suitable for high temperatures of ≤ 24 °C) were acquired from Advantage Moulding, Inc. (ML Lab Friends, Gyeonggido, Korea). Preparation of benzyl chloride standard solution

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Domestication of the novel  - PubMed Central (PMC)
Domestication of the novel - PubMed Central (PMC)

Sep 23, 2019 · Enrichment culture was carried out at 30 °C for 2 weeks in 25-mL serum vials containing 5 mL of the AM medium. The headspace gas was exchanged immediately after inoculation with a synthetic blend gas that mimicked a composition of synthesis gas (50% CO, 10% H 2, 10% CO 2, and 30% N 2; 150 kPa). Whenever positive cultures were identified by an

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Verrucomicrobial methanotrophs grow on  - Nature Research
Verrucomicrobial methanotrophs grow on - Nature Research

Jun 22, 2021 · For comparison, O 2-limited incubations were conducted in 1-L serum vials containing a culture volume of 50 ml supplemented with 10 mM acetone and with 3.5% O 2 (v/v) in the headspace.

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Evaluation of Residual Diazinon and Chlorpiryfos in Children
Evaluation of Residual Diazinon and Chlorpiryfos in Children

Jan 01, 2014 · The optimum sample volume for the headspace extraction of diazinon is 5 mL. Reduction of the solubility of diazinon in the aqueous phase can increase the migration of diazinon to headspace and so the amount of analyte extracted by the fiber, which can do by addition of NaCl. The optimum concentration of NaCl for diazinon extraction was 0.9 g/mL.

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Desulfotomaculum acetoxidans Widdel and Pfennig | ATCC
Desulfotomaculum acetoxidans Widdel and Pfennig | ATCC

The cells can be stored at -70 o C to -80 o C by growing a large volume in #1964 broth, harvesting the cells, and then mixing the cell pellet in an equal volume of fresh #1964 and 20% glycerol (10% final glycerol concentration). Distribute the cells into vials (approximately 0.5 to 1.0 mL per vial), and freeze rapidly.

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C4020-18 - 20ML clear SCREW TOP HDSPACEVIAL ROUND BTM 22X75MM
C4020-18 - 20ML clear SCREW TOP HDSPACEVIAL ROUND BTM 22X75MM

20ML clear SCREW TOP HDSPACEVIAL ROUND BTM 22X75MM, 125/PK, Manufacturer: Thermo Fisher Scientific, Height: 75mm, Volume: 20 ml, Bottle Diameter: 22 mm, Bottle Type: Headspace Vial, Category: Vials JavaScript seems to be disabled in your browser.

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Quantitation of 2-acetyl-1-pyrroline in aseptic-packaged
Quantitation of 2-acetyl-1-pyrroline in aseptic-packaged

Dec 03, 2018 · After fully removing the packaging film, the whole package was transferred to a cutting board and divided into 16 portions (4 columns × 4 rows) with a spatula. After cooling to room temperature for 10 min, 4.0 g of cooked rice was removed and placed in a 20‐ml headspace (HS) vial for SPME extraction.

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A Pulse of Meteoric Subsurface Fluid Discharging Into the
A Pulse of Meteoric Subsurface Fluid Discharging Into the

Jul 19, 2021 · For headspace gas (HS) analyses, 3 ml sediment samples were taken with 5 ml cut-off plastic syringes from the freshly exposed end of each core section and extruded into 30 ml serum glass vials filled with 2 ml of saturated NaCl solution. The HS vials were capped with rubber septa and sealed with aluminum crimp caps.

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ASTM Committee D01 reports of June 2007 subcommittee
ASTM Committee D01 reports of June 2007 subcommittee

Jan 01, 2008 · * The components are mixed, a sample of the mixture is weighed into a 20 mL headspace vial, the vial is sealed with a crimp cap, and the mixture is allowed to cure for 24 to 36 hr at room temperature. After the initial room temperature cure the sample is heated for 30 min at 110[degrees]C.

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Health risk assessment of volatile  - BMC Public Health
Health risk assessment of volatile - BMC Public Health

Apr 20, 2018 · Sorbent in the sampler was transferred to a vial, and 1.5 mL carbon disulphide (CS 2) was added to the vial subsequently. The vial was placed to stand for 45–60 min with occasional stirring for desorption. The extract was then sealed in auto-sampler vials and analyzed by Gas Chromatograph-Mass Selective Detector (GC-MS, Clarus SQ 8 T, Perkin

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Photoautotrophic hydrogen production  - Nature Communications
Photoautotrophic hydrogen production - Nature Communications

Feb 04, 2014 · Photoautotrophic hydrogen production by C. vulgaris YSL01 increased from 0.3 to 0.6 ml l −1 in 3 days as headspace CO 2 Wonju, South Korea ... bottles with a working volume of 250 ml.

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