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In head space gas chromatography, what is actually being tested is the vapor above the minute blood sample in a closed “head space vial.” This form of testing is based on the scientific theory that equilibrium between the substance and the headspace above the substance will be achieved at some point when heated at a constant temperature.
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Solid phase micro-extraction (SPME) headspace sampling, combined with gas chromatography (GC), was used as a reference method. The changes in carrot aroma profiles stored at different temperatures (−18 °C, 4 °C, 25 °C, and 40 °C) were monitored during time up to 26 days.
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Use of headspace–gas chromatography–ion mobility
2019/4/16 · These include proton transfer reaction-mass spectrometry (PTR-MS), gas chromatography–mass spectrometry and headspace solid-phase microextraction (HS-SPME) [12,13,14]. The first used a fingerprinting approach for discerning palm oil by geographical origin, the second intended to identify specific VOCs which contributed to palm oil flavour, whilst the
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2010/4/16 · Static headspace extraction-gas chromatography (SHE-GC) is one of the most commonly used techniques for the analysis of volatile compounds. It is considered by most to be a mature technique and to an extent this is true: there are many users from outside the
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1997/4/15 · Automated headspace-solid-phase micro extraction–retention time locked-isotope dilution gas chromatography–mass spectrometry for the analysis of organotin compounds in water and sediment samples. Journal of Chromatography A 2005 , 1079 (1-2) , 408-414.
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Static Headspace-Gas Chromatography: Theory and
Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique.
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In this work, a simple, precise and accurate static headspace gas chromatography method was developed to investigate the ability of TBT degrading microbes in sedimentary microcosms over a period of 120 days. The proposed method was validated for linearity
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Identification of nitrite treated tuna fish meat via the determination of nitrous oxide by head space-gas chromatography…
calibration: A headspace vial was filled with 5 mL of deionised water and 2 mL of sulphuric acid (20 %), the cap only loosely fitted and the reference gas introduced with a needle through
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